F-5 Whakamatau Fluorine

F-5 Whakamatau Fluorine

Tikanga mahi mo te taputapu ine karewharewha/whakaahua huānga pukoro:

1. Hononga taputapu Tuhonohia te kokoru o te ipu whakakorikori ki te waha o runga o te rotameter me te ngongo silicone, honoa te putanga o te ipu whakakorikori ki te kokoru o te ngongo whakakorikori me te ngongo silicone, ka hono i te putanga o te ngongo whakakorikori. ki te waha o runga o te ngongo condenser me te ngongo silicone hei hono.ka hono te puha wai ki te putanga o te papu wai whakamatao, ka hono te pito o raro o te ngongo condenser ki te puha wai, me te pito o runga o te ngongo condenser e hono ana ki te putanga wai.Tangohia te whakamahana mamaoa, honoa te taura hiko whakamahana, katahi ka kuhu i te pūoko pāmahana capillary ki roto i te aukati rapa, katahi ka kuhua te whakamahana ki roto i te ipu whakamahana.Tangohia te pūoko hauhautanga rakau roa, honoa te pūoko ki te atanga pūoko taputapu ka kuhu ki roto i te uhi whakawera oumu hiko.I tenei wa, ka hono te taputapu.

2. Te patuiro taputapu: Tāpirihia te 900 mL wai ki te ipu whakamahana hei kati i te aukati rapa whakamahana, hoatu te 5 mL o te whakamaroke ki roto i te ngongo whakamaarama kiripaka, ka hono i nga hononga ngongo silicone katoa.

3. Whakakā I mua i te whakakā i te mihini, tuatahi tirohia mena he wai whakamatao kei waho, kuhuna te mono hiko o te taputapu ki roto i te turanga, whakahurihia te pana hiko, whakahurihia te wai whakamatao, ka kite mena kua ki tonu te ngongo condensate. o te condensate me hoki ki te taika wai.Whakaturia te pāmahana e whakahaeretia ana e te whakamaarama ki te 250 ℃, whakakāhia te whakakā whakawera me te whakakā papu hau, me te whakatika i te puku o te karaka ki te tautuhi i te huringa pāmahana ki te 110 ℃.I muri i te whewhe o te wai i roto i te ipu whakamaaratanga, whakatikahia te puku whakamahana ki te taha karaka kia noho te wai ki te 85 ℃.Ae, whakatikahia te mita rere hau, whakahaere i te rere o te hau ki te 100 ─ 150 mL/mene, me te whakamarumaru mo te 2 meneti I muri i te karaka, tirohia mena kei te rere mai te distillate mai i te ngongo condenser.Mena kei reira, he mea noa.Ki te kore, tirohia koa mehemea he pai te hono o te paipa, he pai te hono o te hiko whakawera.

4. Whakaweto Ko te raupapa whakaweto ko: whakawetohia te whakamahana─whakawetohia te papu hau─whakawetohia te papu wai whakamatao─whakawetohia te mana hiko─tangohia te mono hiko─mutunga.

Kaitātari huānga pūkōkōkore Te tiaki i te mita pūkōkōkore:

1. Me whakahaere te whakahinuhinu kia rite ki nga waahanga whakahinuhinu kua tohua me nga tikanga whakahinuhinu i mua i te tiimata o te miihini.

2. Te whakakore me te huihuinga e nga tohunga e mohio ana ki te hanganga o te miihini whakamatautau.

3. I te wa kaore te miihini whakamatautau mo te wa roa, me whakakikoruatia ki te hinu anti-waikura i runga i te mata mahi ka rongoa ki te waahi maroke.

4. Kia ma te miihini whakamatautau.

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Tōmua: Taiwhanga Roopu Whakawera Tonu me te Kaiwhakahaere Mamati

Panuku: Rere Rere Waahanga Kaiwhakamatau Ihirangi

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